Chemistry and Chemical Engineering Research Center of Iran P.O.Box 14335-186, Tehran, Iran
Abstract
A room-temperature procedure is developed for the direct synthesis of monoarylidene derivatives of pyran-4-one and piperidin-4-one systems under solvent-free conditions. Relatively high yields of products are obtained from the reaction of ketones 1 with different aromatic and aliphatic aldehydes under the catalytic system of TMSNMe2 and MgBr2·OEt2. Notably, formation of the undesired bis counterparts as a major limitation of these reaction types, is minimized using the employed conditions.
Mojtahedi, M. M., Abaee, M. S., Samianifard, M. & Shamloo, A. (2014). An efficient synthesis of monoarylidene derivatives of pyran-4-one and piperidin-4-one. Scientia Iranica, 21(3), 719-726.
MLA
Mojtahedi, M. M., Abaee, M. S., Samianifard, M., & Shamloo, A. "An efficient synthesis of monoarylidene derivatives of pyran-4-one and piperidin-4-one", Scientia Iranica, 21, 3, 2014, 719-726.
HARVARD
Mojtahedi M. M., Abaee M. S., Samianifard M., Shamloo A. (2014). 'An efficient synthesis of monoarylidene derivatives of pyran-4-one and piperidin-4-one', Scientia Iranica, 21(3), pp. 719-726.
CHICAGO
M. M. Mojtahedi, M. S. Abaee, M. Samianifard & A. Shamloo, "An efficient synthesis of monoarylidene derivatives of pyran-4-one and piperidin-4-one," Scientia Iranica, 21 3 (2014): 719-726,
VANCOUVER
Mojtahedi M. M., Abaee M. S., Samianifard M., Shamloo A. An efficient synthesis of monoarylidene derivatives of pyran-4-one and piperidin-4-one. Scientia Iranica. 2014;21(3):719-726.
